- BRUKER EPR STANDARDS FULL
- BRUKER EPR STANDARDS PLUS
Time Required for NMR Experiments on A500a: Mass Time Required for NMR Experiments on A400c: MassĢ channel system, OneNMR probe with auto-tune-and-match installed.
2D HSQC and HMBC experiments (night time). Primarily used for short, routine NMR experiments where data is needed quickly. Time Required for NMR Experiments on A400b: MassĢ channel system with AS7620 96-sample changer. OneNMR probe with auto-tune-and-match installed. Variable Temperature experiments (with appropriate CBIC training). Simultaneous F19 and H1 experiments (i.e. F19 with H1 decoupling). Variable-temperature and H/F experiments available. Time Required for NMR Experiments on A400a: MassĪll estimates based on a 500 MW sample in 600 uL solvent volume using a 5 mm diameter NMR tubeĢ channel system. AutoX DB probe installed. Other nuclei: F19 (no H1 decoupling), P31, B11, (others by request). 
Undergraduates have priority on this instrument during lab periods. Probe with auto-tune-and-match installed. This is a good way to discover other equipment on campus that might be useful to proposals.2 channel system with AS7620 96-sample changer.
UW-Madison’s Resource Directory provides a searchable database to over 90 campus core instrumentation facilities. Other resources on the UW-Madison campus: The Department also has an Electronics Shop, Glass Shop, and Instrument (Machine) Shop with links on the same page. Catalysis Center, Keck Center and Laboratory, and High-Performance Computing Center have links here. Other equipment in the Chemistry Department: Bruker D8 Advance powder diffractometer with a Cu Kα conventional sealed X-ray tube and Lynxeye detector. Bruker SMART APEX2 single-crystal diffractometer with a Cu Kα conventional sealed X-ray tube with Oxford Cryosystems 700 low temperature device. Bruker Quazar APEX2 single-crystal diffractometer with a Mo Kα IµS radiation source and Oxford Cryosystems 700 low temperature device. SeeCo Mössbauer Spectrometry W304 and W204. Shimadzu GCMS-QP2010S (GC-EI-single quad-MS). Bruker ultraFlex III (MALDI-TOF/TOF-MS). BRUKER EPR STANDARDS PLUS
Thermo Scientific Q Exactive Plus (ESI-Q-orbitrap-MS). Bruker EleXsys EPR - very high sensitivity EPR with ER 049SX SuperX Bridge and SuperX, Double Rectangular, and Dual Mode Cavities. Bruker AVANCE 600 - houses the Center for Laser-Assisted NMR: Bruker TCI-F LHe-cooled cryoprobe and autosampler interfaced to Coherent Inova Sabre DBW25 Laser, Coherent Chameleon Ultra Laser, and Ultra High Power LED-450 and 405 light sources. Bruker AVANCE 500(b) - state-of-the-art 13C capabilities with Bruker DCH LHe-cooled cryoprobe autosampler. Bruker AVANCE 500(a) - state-of-the-art direct-X detection with Bruker Prodigy BB LN2-cooled probe extensive kinetics and dynamics capabilities (Smartprobe) triple resonance 19F-13C-1H experiments (FCH probe) Solid-State NMR with Bruker MAS3 controller Doty 4mm DI-4 1H/X/Y B MAX solids MAS probe PhoenixNMR 1.2mm 1H/X/Y MAS probe PhoenixNMR 5mm UltraWideline 1H/X static probe autosampler. 
Bruker AVANCE 400(b) - state-of-the-art high-throughput capabilities directed toward synthetic research progress with Bruker SampleJet sample changer plus BBFO+ probe. Bruker AVANCE 400(a) - state-of-the-art high-throughput capabilities directed toward undergraduate education and research training with Bruker SampleJet sample changer plus BBFO+ probe. Bruker AVANCE 360 - houses the Wisconsin High-Pressure NMR Reactor system (WiHP-NMRR) broadband capabilities, variable temperature with gas pressures in excess of 1000psi. Varian MercuryPlus 300 - standard NMR with rapid access and auto-sampler. BRUKER EPR STANDARDS FULL
Full time staff members are available to assist graduate students and post doctoral associates with the design and fabrication of specialized equipment for experiments.
The Department also has an in house electronics shop, machine shop, glass shop and an instrumentation shop. Samuel Gellman, and is maintained by a staff of six Ph.D. The chemistry department has shared facilities in our Chemical Instrumentation Center (CIC) for EPR (Bruker EleXsys EPR: E-500-A console with ER 049SX SuperX Bridge SuperX or Double Rectangular or Dual Mode Cavity), mass spectrometry (Bruker ULTRAFLEX III, Bruker REFLEX II, Waters AutoSpec, Waters LCT, Shimadzu LCMS-2010A, Shimadzu GCMS-QP2010S), Mössbauer (SeeCo Mössbauer Spectrometry with Janis SHI-850 4K Cryostat), NMR (Varian Mercury Plus 300, Bruker AVANCE 360, two Bruker AVANCE III 400, two Bruker AVANCE III 500, Bruker AVANCE III 600), X-ray diffraction (Bruker Quazar APEX2 with a Mo Kα IµS radiation source and Bruker SMART APEX2 with a Cu Kα conventional sealed X-ray tube with Oxford Cryosystems low temperature devices Bruker D8 Advance with a Cu Kα conventional sealed X-ray tube and Lynxeye detector) and SQUID Megnetometer (Quantum Design MPMS3 EverCool System).
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